Metal 430 - Fall 2000

Tentative Course Schedule

August 22

 

 

General
Nature of materials characterization -
morphology, chemistry, etc.
Techniques for bulk characterization
Techniques for surface characterization

August 24

 

 

 

 

 

X-ray diffraction
Nature and production of x-rays
Bragg's law and diffraction patterns
Instrument
Specimen preparation
Qualitative analysis - the PDF
Industrial examples
Four-circle diffractometry

September 14

 

 

 

 

X-ray fluorescence
Purpose
General characteristics
Wavelength dispersive instrument
Energy dispersive instrument
Industrial example

September 21

 

 

 

 

 

 

Optical microscopy
Optics
Lenses and image formation
Depth of field
Numerical aperture
Resolution
Instrument
Specimen preparation
Contrast
Examples

 October 3

 

 

Electron microscopy
Electron sources, acceleration, and focusing
Scanning electron microscopy
Transmission electron microscopy

 October 19

 

 

 

 

Chemical analysis in electron microscopes
Electron-atom interactions
Energy-dispersive spectroscopy
Wavelength-dispersive spectroscopy / electron
microprobe
Electron energy loss spectroscopy

 October 26

 

 

 

 

 

Surface and thin film analysis
Profilometry
Scanning probe microscopies
Scanning tunneling microscopy
Atomic force microscopy
X-ray photoelectron spectroscopy
Auger electron spectroscopy
Secondary ion mass spectroscopy
Rutherford backscattering spectrometry

 November 28

 

 

 

 

Infrared spectroscopy
Molecular vibrations
Nature of spectrum
The Fourier transform and Interferograms
The interferometer
Instrument
Specimen preparation
Examples

December 7

 

Course summary and wrap-up